Osaka Soda (Shiseido) / Capcell PAK

Capcell PAK

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Capcell-Pak HPLC columns are manufactured by Osaka-Soda in Japan. Previously, the columns belonged to the Shiseido Company, whose chromatography division was acquired by Osaka Soda in 2017. The base silica is first homogeneously coated with a silicone polymer monolayer, by vapour deposition. A series of phases is then produced by bonding alkyl groups, which shield any acidic silanols, to the coated surface. This imparts superior mechanical strength as well as extended pH stability. The product line has evolved over time with regard to quality of the silica support as well as the polymer coating technology. All phases, except the Capcell-Pak AG series, are based on high purity Type B silica gel.

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Technical Data

Capcell-Pak AG Series

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18 AG

C18

5 µm

120 Å

Polymer coating

15%

L1

300m2/g

2.0-10.0

N/A

Capcell Pak C8 AG

C8

5 µm

120 Å

Polymer coating

9%

L7

300m2/g

2.0-10.0

N/A

Capcell-Pak SG Series ("Special-Grade)

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18
SG 120

C18

3, 5 µm

120 Å

Polymer coating

15%

L1

300m2/g

2.0-9.0

N/A

Capcell Pak C18
SG 300

C18

5 µm

300 Å

Polymer coating

10%

L1

150m2/g

2.0-9.0

N/A

Capcell Pak C8
SG 300

C8

5 µm

300 Å

Polymer coating

6%

L7

150m2/g

2.0-9.0

N/A

Capcell Pak C1
SG 300

C1

5 µm

300 Å

Polymer coating

3%

L13

150m2/g

2.0-9.0

N/A

Capcell Pak Ph
SG 120

phenyl

5 µm

120 Å

Polymer coating

7%

L1

300m2/g

2.0-9.0

N/A

Capcell Pak CN
SG 120

Cyano (CN)

5 µm

120 Å

Polymer coating

6%

L10

300m2/g

2.0-9.0

N/A

Capcell Pak NH2
SG 80

Amino (NH2)

5 µm

80 Å

Polymer coating

14%

L8

450m2/g

2.0-8.0

N/A

Capcell-Pak UG Series ("Ultra-Grade")

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18
UG 80

C18

5 µm

80 Å

Polymer coating

18%

L1

300m2/g

2.0-10.0

N/A

Capcell Pak C18
UG 120

C18

3, 5 µm

120 Å

Polymer coating

15%

L1

300m2/g

2.0-10.0

N/A

Capcell Pak C8
UG 120

C8

5 µm

120 Å

Polymer coating

9%

L7

300m2/g

2.0-10.0

N/A

Capcell Pak C1
UG 120

C1

5 µm

120 Å

Polymer coating

4%

L13

300m2/g

2.0-10.0

N/A

Capcell Pak Ph
UG 120

phenyl

5 µm

120 Å

Polymer coating

8%

L1

300m2/g

2.0-10.0

N/A

Capcell Pak CN
UG 120

Cyano (CN)

5 µm

120 Å

Polymer coating

5%

L10

300m2/g

2.0-10.0

N/A

Capcell Pak NH2
UG 80

Amino (NH2)

5 µm

80 Å

Polymer coating

14%

L8

450m2/g

2.0-8.0

N/A

Capcell Pak SCX
UG 80

Sulphonic acid

5 µm

80 Å

Polymer coating

9%

L9

450m2/g

2.0-7.0

N/A

Capcell-Pak MG Series

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18
MG

C18

3, 5 µm

100 Å

Polymer coating

15%

L1

300, 260m2/g

2.0-10.0

N/A

Capcell Pak C18
MG II

C18

3, 5 µm

100 Å

Polymer coating

15%

L1

300, 260m2/g

2.0-10.0

N/A

Capcell Pak C18
MG III

C18

2 µm
3, 5 µm

100 Å

Polymer coating

15%

L1

300, 260m2/g

2.0-10.0

N/A

Capcell-Pak IF Series ("Ideally Fine")

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18 IF

C18

2 µm

120 Å

Polymer coating

14%

L1

340m2/g

2.0-9.0

N/A

Capcell Pak C18 IF2

C18

2.2 µm

80 Å

Polymer coating

15.5%

L1

480m2/g

2.0-9.0

N/A

Capcell-Pak ACR Series ("Acidic Resistance")

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18 ACR

C18

3, 5 µm

80 Å

Polymer coating

17%

L1

300m2/g

1.0-10.0

N/A

Capcell-Pak AQ Series (100% Aqueous compatible)

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18 AQ

C18

3 µm

80 Å

Polymer coating

12%

L1

330m2/g

2.0-9.0

N/A

Capcell Pak C18 AQ

C18

5 µm

80 Å

Polymer coating

11%

L1

300m2/g

2.0-9.0

N/A

Capcell-Pak DD Series ("Double Durability")

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C8 DD

C8

3, 5 µm

80 Å

Polymer coating

11%

L7

300m2/g

1.5-10.0

N/A

Capcell-Pak BB Series (Alkali Resistance Column)

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak C18 BB

C18

3, 5 µm

130 Å

Polymer coating

17%

L1

300m2/g

1.0-11.0

N/A

Capcell-Pak CR Series (Strong Cation Exchange & Reversed Phase)

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak CR

SCX + C18

3, 5 µm

N/A

N/A

N/A

N/A

N/A

N/A

N/A

Capcell-Pak ADME Series

Phase name

Modification

Particle size

Pore size

End-capping

C-content

USP

Surface area

pH range

Tmax

Capcell Pak ADME

Adamantyl

2, 3, 5 µm

100 Å

Polymer coating

12%

N/A

300 m2/g

2.0-9.0

N/A

Capcell Pak ADME-HR

Adamantyl

2, 3, 5 µm

100 Å

N/A

12%

N/A

310 m²/g

2.0-9.0

N/A

Capcell Pak INERT ADME-HR

Adamantyl

3 µm

100 Å

N/A

12%

N/A

310 m²/g

2.0-9.0

N/A

Applications

CAPCELL PAK C18 AQ S3 Acrylamide

Determination of acrylamide with CAPCELL PAK C18 AQ S3.

1. acrylamide

Test Conditions:

Column: CAPCELL PAK C18 AQ S3 ; 2.0 mm i.d. x 150 mm

Mobile Phase: 0.1 vol% HCOOH / CH3OH = 98.5 / 1.5

Flow rate: 200 μL/min

Temperature: 30°C

Detection: LC-MS/MS (SRM : Selected Reaction Monitoring)

Ionization: ESI +

Injection volume: 5 µL

Sample: dissolved in mobile phase

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